- Turkish Journal of Chemistry
- Vol: 38 Issue: 5
- Graphene oxide--magnetite nanocomposite as an efficient and magnetically separable adsorbent for met...
Graphene oxide--magnetite nanocomposite as an efficient and magnetically separable adsorbent for methylene blue removal from aqueous solution
Authors : Kadem Meral, Önder Metin
Pages : 775-782
Doi:10.3906/kim-1312-28
View : 9 | Download : 5
Publication Date : 9999-12-31
Article Type : Makaleler
Abstract :We report a facile method to produce a magnetically separable graphene oxide--magnetite nanocomposite (GO--Fe3O4) and its adsorption performance in methylene blue (MB) removal from aqueous solution. The GO--Fe3O4 nanocomposite was synthesized by a solution-phase self-assembly method including the incorporation of monodisperse Fe3O4 nanoparticles (NPs) and GO in a dimethylformamide/chloroform mixture under sonication. The successfully decorating GO sheet with monodisperse Fe3O4 NPs was proved by TEM study. ICP--OES data of the GO--Fe3O4 nanocomposite show that the GO--Fe3O4 nanocomposite consists of 21 wt% Fe3O4 NPs, which is sufficient for its magnetic separation from aqueous solution. The spectroscopic studies reveal that the GO--Fe3O4 nanocomposite is a highly efficient adsorbent for MB removal from aqueous solution, providing an adsorption capacity of 172.6 mg/g, and the equilibrium for MB adsorption is attained in \sim 70 min. Moreover, it is a magnetically separable and reusable material for MB removal from water, preserving 87% of its initial efficiency after 5 successive runs.Keywords : Graphene oxide, Fe3O4 nanoparticles, composite sorbent, magnetic separation, dye removal, methylene blue